About Energy storage lithium battery agent
G3 solvent (Sigma Aldrich, >99%) was dried over freshly activated 4 Å molecular sieves for several days. LiTFSI (purity >98%, Wako Chemicals) and LiFSI (purity >99%, Wako Chemicals) were dried by heating under.
Li2O was obtained from lithium peroxide (Li2O2, Alfa Aesar) by thermal decomposition. In detail, L.
The electrodes were assembled into a 2032 coin cell (Hohsen). The half cell was assembled by successively stacking a lithium foil anode (thickness, 0.4 mm), a glass fibre filter (.
High-resolution TEM (HR-TEM) images were obtained using a JEM-2100 (HR) electron microscope. For the HR-TEM observations, the powders were subjected to ultrasound tre.
The in situ Raman spectra were recorded using a JASCO microscope spectrometer (NRS-1000DT). The 632.8-nm excitation light of an air-cooled HeNe laser was focused on the el.
A homemade cell for in situ online DEMS and a custom-built glass vessel for ex situ gas chromatography mass spectrometry were connected to an eight-port, two-way gas chromatogra.
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